Information card for entry 7062958

Structure parameters

• Formula: C126 H164 Dy0.09 N20 Ni4 O54 Y3.91
• Calculated formula: C116 H100 Dy0.064 N20 Ni4 O32 Y3.936
• Title of publication: Synthesis, crystal structure and magnetic properties of octanuclear Ni4Ln4 complexes constructed using a Schiff base ligand and di-2-pyridyl ketone
• Authors of publication: Zhu, Yu-Jie; Wang, Hui-Sheng; Chen, Yuxiang; Zhou, Pengfei; Wu, Yanfang; Zhang, Yi-Quan
• Journal of publication: New Journal of Chemistry
• Year of publication: 2024
• Journal volume: 48
• Journal issue: 8
• Pages of publication: 3438 - 3446
• a: 48.0558 ± 0.0015 Å
• b: 19.4125 ± 0.0006 Å
• c: 15.7368 ± 0.0004 Å
• α: 90°
• β: 99.265 ± 0.001°
• γ: 90°
• Cell volume: 14489.1 ± 0.7 ų
• Cell temperature: 172 ± 2 K
• Ambient diffraction temperature: 172 ± 2 K
• Number of distinct elements: 7
• Space group number: 15
• Hermann-Mauguin space group symbol: C 1 2/c 1
• Hall space group symbol: -C 2yc
• Residual factor for all reflections: 0.0989
• Residual factor for significantly intense reflections: 0.0565
• Weighted residual factors for significantly intense reflections: 0.1628
• Weighted residual factors for all reflections included in the refinement: 0.1832
• Goodness-of-fit parameter for all reflections included in the refinement: 1.099
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No