Information card for entry 7063011

Structure parameters

• Formula: C22 H28 F6 P Rh
• Calculated formula: C22 H28 F6 P Rh
• Title of publication: Catalytic activity of cyclobutadiene rhodium complexes in hydrosilylation and other transformations of alkynes
• Authors of publication: Petrushina, Tatiana N.; Nelyubina, Yulia V.; Perekalin, Dmitry S.; Shvydkiy, Nikita V.
• Journal of publication: New Journal of Chemistry
• Year of publication: 2024
• Journal volume: 48
• Journal issue: 9
• Pages of publication: 3952 - 3956
• a: 15.909 ± 0.0014 Å
• b: 17.5486 ± 0.0017 Å
• c: 15.8848 ± 0.0016 Å
• α: 90°
• β: 90.557 ± 0.006°
• γ: 90°
• Cell volume: 4434.5 ± 0.7 ų
• Cell temperature: 100 K
• Ambient diffraction temperature: 100 K
• Number of distinct elements: 5
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/c 1
• Hall space group symbol: -P 2ybc
• Residual factor for all reflections: 0.0978
• Residual factor for significantly intense reflections: 0.084
• Weighted residual factors for significantly intense reflections: 0.2455
• Weighted residual factors for all reflections included in the refinement: 0.2683
• Goodness-of-fit parameter for all reflections included in the refinement: 1.038
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No