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Information card for entry 7063049
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Coordinates | 7063049.cif |
---|---|
Original paper (by DOI) | HTML |
Formula | C30 H21 F6 N5 O Pd |
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Calculated formula | C30 H21 F6 N5 O Pd |
Title of publication | Guanidine-centred reactivity of CNN Pd(ii) pincer complexes including carboxylate-assisted N–H activation and –CH2– → –C(O)– oxygenation |
Authors of publication | Sinha, Nitish Kumar; Khan, Hilal Ahmad; Sivasankar, Chinnappan; Thirupathi, Natesan |
Journal of publication | New Journal of Chemistry |
Year of publication | 2024 |
Journal volume | 48 |
Journal issue | 13 |
Pages of publication | 5710 - 5720 |
a | 8.4101 ± 0.0005 Å |
b | 11.9592 ± 0.0003 Å |
c | 14.4653 ± 0.0003 Å |
α | 82.43 ± 0.002° |
β | 74.423 ± 0.004° |
γ | 72.257 ± 0.004° |
Cell volume | 1332.82 ± 0.1 Å3 |
Cell temperature | 204 ± 60 K |
Ambient diffraction temperature | 204 ± 60 K |
Number of distinct elements | 6 |
Space group number | 2 |
Hermann-Mauguin space group symbol | P -1 |
Hall space group symbol | -P 1 |
Residual factor for all reflections | 0.0498 |
Residual factor for significantly intense reflections | 0.0417 |
Weighted residual factors for significantly intense reflections | 0.0946 |
Weighted residual factors for all reflections included in the refinement | 0.0995 |
Goodness-of-fit parameter for all reflections included in the refinement | 0.992 |
Diffraction radiation probe | x-ray |
Diffraction radiation wavelength | 0.71073 Å |
Diffraction radiation type | MoKα |
Has coordinates | Yes |
Has disorder | No |
Has Fobs | No |
For the version history of this entry, please navigate to main COD server.
The link is: https://www.crystallography.net/7063049.html
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Users of the data should acknowledge the original authors of the
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