Information card for entry 7063069

Structure parameters

• Formula: C22 H30 Cl4 F2 N8 P4
• Calculated formula: C22 H30 Cl4 F2 N8 P4
• Title of publication: Phosphorus–nitrogen compounds. Part 73. Dispiromono and dispirobicyclotetraphosphazene derivatives: syntheses, and spectroscopic, crystallographic and thermal studies
• Authors of publication: Elmas, Gamze; Okumuş, Aytuğ; Kılıç, Zeynel; Hökelek, Tuncer
• Journal of publication: New Journal of Chemistry
• Year of publication: 2024
• Journal volume: 48
• Journal issue: 13
• Pages of publication: 5804 - 5819
• a: 9.1703 ± 0.0003 Å
• b: 9.7421 ± 0.0003 Å
• c: 9.8703 ± 0.0004 Å
• α: 74.561 ± 0.004°
• β: 82.14 ± 0.004°
• γ: 63.676 ± 0.003°
• Cell volume: 761.65 ± 0.05 ų
• Cell temperature: 173 ± 2 K
• Ambient diffraction temperature: 173 ± 2 K
• Number of distinct elements: 6
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0402
• Residual factor for significantly intense reflections: 0.0379
• Weighted residual factors for significantly intense reflections: 0.1002
• Weighted residual factors for all reflections included in the refinement: 0.102
• Goodness-of-fit parameter for all reflections included in the refinement: 1.066
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No