Crystallography Open Database

Information card for entry 7063106

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Coordinates	7063106.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C20 H17 N O4 S
Calculated formula	C20 H17 N O4 S
Title of publication	Rh(iii)-catalyzed sequential spiroannulation/lactonization of 3-aryl N-sulfonyl ketimines with 4-hydroxy-2-alkynoates by C–H bond activation
Authors of publication	Prashanth, S.; Ajay, Chidrawar; Nagesh, Kommu; Sridhar, B.; Reddy, B. V. Subba
Journal of publication	New Journal of Chemistry
Year of publication	2024
Journal volume	48
Journal issue	17
Pages of publication	7646 - 7650
a	11.908 ± 0.002 Å
b	10.3611 ± 0.0019 Å
c	14.976 ± 0.002 Å
α	90°
β	97.885 ± 0.007°
γ	90°
Cell volume	1830.3 ± 0.5 Å³
Cell temperature	294 ± 2 K
Ambient diffraction temperature	294 ± 2 K
Number of distinct elements	5
Space group number	14
Hermann-Mauguin space group symbol	P 1 21/c 1
Hall space group symbol	-P 2ybc
Residual factor for all reflections	0.0618
Residual factor for significantly intense reflections	0.0415
Weighted residual factors for significantly intense reflections	0.1042
Weighted residual factors for all reflections included in the refinement	0.1174
Goodness-of-fit parameter for all reflections included in the refinement	1.037
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

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