Information card for entry 7063255

Structure parameters

• Formula: C29 H26
• Calculated formula: C29 H26
• Title of publication: Unexpectedly Superior Efficiency of Chloride-directed Double Suzuki-Miyaura Cross-coupling Reaction to That of Bromide for the Synthesis of Sterically Hindered 2,7-Diaryl Fluorenes
• Authors of publication: Peng, Yuqing; Li, Yongqing; liu, maomao; Ni, Chen; Cao, Yucai
• Journal of publication: New Journal of Chemistry
• Year of publication: 2024
• a: 7.944 ± 0.002 Å
• b: 11.109 ± 0.003 Å
• c: 13.45 ± 0.004 Å
• α: 70.038 ± 0.014°
• β: 75.929 ± 0.015°
• γ: 76.156 ± 0.014°
• Cell volume: 1066.2 ± 0.5 ų
• Cell temperature: 193 ± 2 K
• Ambient diffraction temperature: 193 ± 2 K
• Number of distinct elements: 2
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.1592
• Residual factor for significantly intense reflections: 0.1416
• Weighted residual factors for significantly intense reflections: 0.3521
• Weighted residual factors for all reflections included in the refinement: 0.3692
• Goodness-of-fit parameter for all reflections included in the refinement: 1.563
• Diffraction radiation wavelength: 1.34139 Å
• Diffraction radiation type: GaKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No