Information card for entry 7063284

Structure parameters

• Formula: C12 H16 Cl2 N8 Ni O16
• Calculated formula: C12 H16 Cl2 N8 Ni O16
• Title of publication: The new dual anion solvent-free nickel complex based on the pyridine-4-carbohydrazide ligand
• Authors of publication: Kuang, Bao-long; Zhao, Bin-shan; Lu, Zu-jia; Wang, Ting-wei; Xie, Zhi-ming; Sun, Mou; Yu, Qi-yao; Zhang, Jian-guo
• Journal of publication: New Journal of Chemistry
• Year of publication: 2024
• Journal volume: 48
• Journal issue: 29
• Pages of publication: 12873 - 12876
• a: 10.1017 ± 0.0004 Å
• b: 15.6632 ± 0.0007 Å
• c: 14.8448 ± 0.0008 Å
• α: 90°
• β: 105.269 ± 0.005°
• γ: 90°
• Cell volume: 2265.9 ± 0.19 ų
• Cell temperature: 120.65 ± 0.1 K
• Ambient diffraction temperature: 120.65 ± 0.1 K
• Number of distinct elements: 6
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/c 1
• Hall space group symbol: -P 2ybc
• Residual factor for all reflections: 0.0593
• Residual factor for significantly intense reflections: 0.045
• Weighted residual factors for significantly intense reflections: 0.1012
• Weighted residual factors for all reflections included in the refinement: 0.1115
• Goodness-of-fit parameter for all reflections included in the refinement: 1.039
• Diffraction radiation probe: x-ray
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No