Information card for entry 7063343

Structure parameters

• Formula: C16 Cs4 N16 O W2
• Calculated formula: C16 Cs4 N16 O W2
• Title of publication: Synthesis of diaminoacetylene from cyanido ligands of the octacyanidotungstate complex
• Authors of publication: Szklarzewicz, Janusz; Hodorowicz, Maciej; Jurowska, Anna
• Journal of publication: New Journal of Chemistry
• Year of publication: 2024
• Journal volume: 48
• Journal issue: 29
• Pages of publication: 13196 - 13205
• a: 11.8245 ± 0.0003 Å
• b: 8.6678 ± 0.0002 Å
• c: 14.9294 ± 0.0004 Å
• α: 90°
• β: 98.581 ± 0.002°
• γ: 90°
• Cell volume: 1513.02 ± 0.07 ų
• Cell temperature: 100 ± 2 K
• Ambient diffraction temperature: 100 ± 0.1 K
• Number of distinct elements: 5
• Space group number: 7
• Hermann-Mauguin space group symbol: P 1 c 1
• Hall space group symbol: P -2yc
• Residual factor for all reflections: 0.0359
• Residual factor for significantly intense reflections: 0.0348
• Weighted residual factors for significantly intense reflections: 0.0837
• Weighted residual factors for all reflections included in the refinement: 0.0846
• Goodness-of-fit parameter for all reflections included in the refinement: 1.011
• Diffraction radiation probe: x-ray
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No