Crystallography Open Database

Information card for entry 7101239

Preview

Coordinates	7101239.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C52 H68 Co2 N3 O5.5 P3
Calculated formula	C51.96 H67.92 Co2 N3 O5.49 P3
Title of publication	Reactivity of Electrophilic m-Phosphinidene Complexes with N-Heterocyclic Carbenes: Formation of the First Main Group Element Adducts of 'Abnormal Carbene' Ligands.
Authors of publication	A. Carty; Todd Graham; Konstantin A. Udachin
Journal of publication	Chemical Communications
Year of publication	2006
Journal issue	25
a	11.2872 ± 0.001 Å
b	11.6939 ± 0.001 Å
c	20.7381 ± 0.0018 Å
α	89.924 ± 0.001°
β	74.93 ± 0.001°
γ	75.553 ± 0.001°
Cell volume	2553.6 ± 0.4 Å³
Cell temperature	125 ± 2 K
Ambient diffraction temperature	125 ± 2 K
Number of distinct elements	6
Space group number	2
Hermann-Mauguin space group symbol	P -1
Hall space group symbol	-P 1
Residual factor for all reflections	0.0492
Residual factor for significantly intense reflections	0.0345
Weighted residual factors for significantly intense reflections	0.0893
Weighted residual factors for all reflections included in the refinement	0.0996
Goodness-of-fit parameter for all reflections included in the refinement	1.053
Diffraction radiation wavelength	0.7107 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

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