Information card for entry 7101456

Structure parameters

• Formula: C43 H84 I O P2 Rh
• Calculated formula: C43 H84 I0.9972 O P2 Rh
• Title of publication: Gyroscope-Like Molecules Consisting of Three-Spoke Stators that Enclose Switchable Neutral Dipolar Rhodium Rotators; Reversible Cycling between Faster and Slower Spinning Rh(CO)I and Rh(CO)2I Species
• Authors of publication: J.Gladysz; Frank Hampel; Takanori Shima; Leyong Wang.
• Journal of publication: Chemical Communications
• Year of publication: 2006
• Journal issue: 39
• a: 23.4154 ± 0.0004 Å
• b: 12.3194 ± 0.0003 Å
• c: 34.0731 ± 0.0008 Å
• α: 90°
• β: 109.066 ± 0.001°
• γ: 90°
• Cell volume: 9289.7 ± 0.4 ų
• Cell temperature: 173 ± 2 K
• Ambient diffraction temperature: 173 ± 2 K
• Number of distinct elements: 6
• Space group number: 15
• Hermann-Mauguin space group symbol: C 1 2/c 1
• Hall space group symbol: -C 2yc
• Residual factor for all reflections: 0.1181
• Residual factor for significantly intense reflections: 0.0494
• Weighted residual factors for significantly intense reflections: 0.1051
• Weighted residual factors for all reflections included in the refinement: 0.1433
• Goodness-of-fit parameter for all reflections included in the refinement: 0.947
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No