Information card for entry 7101484

Structure parameters

• Formula: C74 H148 B2 Cl4 F8 N8 S24 V4
• Calculated formula: C74 H148 B2 Cl4 F8 N8 S24 V4
• Title of publication: Highly-Oxidised, Sulfur-Rich, Mixed-Valence Vanadium(IV/V) Complexes
• Authors of publication: C. Young; David J. Evans; Michelle K. Taylor
• Journal of publication: Chemical Communications
• Year of publication: 2006
• Journal issue: 40
• a: 14.7389 ± 0.0013 Å
• b: 20.7238 ± 0.0018 Å
• c: 21.4366 ± 0.0018 Å
• α: 79.133 ± 0.002°
• β: 76.828 ± 0.002°
• γ: 73.115 ± 0.002°
• Cell volume: 6047.8 ± 0.9 ų
• Cell temperature: 130 ± 2 K
• Ambient diffraction temperature: 130 ± 2 K
• Number of distinct elements: 8
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.1386
• Residual factor for significantly intense reflections: 0.0813
• Weighted residual factors for significantly intense reflections: 0.1991
• Weighted residual factors for all reflections included in the refinement: 0.226
• Goodness-of-fit parameter for all reflections included in the refinement: 0.976
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No