Crystallography Open Database

Information card for entry 7101504

Preview

Coordinates	7101504.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C162.5 H142 B4 Cl6 F16 N4 O4 P8 Rh4 S4
Calculated formula	C162.5 H142 B4 Cl6 F16 N4 O4 P8 Rh4 S4
Title of publication	Tetrametallic Rectangular Box Complexes Assembled from Heteroligated Macrocycles
Authors of publication	Chad Mirkin; Aaron M. Brown; Maxim V. Ovchinnikov; Charlotte L. Stern
Journal of publication	Chemical Communications
Year of publication	2006
Journal issue	42
a	17.6443 ± 0.0014 Å
b	21.5365 ± 0.0017 Å
c	24.3009 ± 0.0019 Å
α	73.616 ± 0.001°
β	75.764 ± 0.001°
γ	88.215 ± 0.001°
Cell volume	8580 ± 1.2 Å³
Cell temperature	153 ± 2 K
Ambient diffraction temperature	153 ± 2 K
Number of distinct elements	10
Space group number	2
Hermann-Mauguin space group symbol	P -1
Hall space group symbol	-P 1
Residual factor for all reflections	0.1391
Residual factor for significantly intense reflections	0.0987
Weighted residual factors for significantly intense reflections	0.2883
Weighted residual factors for all reflections included in the refinement	0.326
Goodness-of-fit parameter for all reflections included in the refinement	1.192
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

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