Information card for entry 7101848

Structure parameters

• Formula: C37.6 H46.4 Cl2 N4 Sb2
• Calculated formula: C37.6 H46.4 Cl2 N4 Sb2
• Title of publication: Diamidonaphthalene-supported pnictogenium cations: synthesis of an N-heterocyclic stibenium cation by a novel protonation route.
• Authors of publication: Spinney, Heather A; Korobkov, Ilia; Richeson, Darrin S
• Journal of publication: Chemical communications (Cambridge, England)
• Year of publication: 2007
• Journal issue: 16
• Pages of publication: 1647 - 1649
• a: 15.669 ± 0.004 Å
• b: 11.931 ± 0.003 Å
• c: 21.118 ± 0.005 Å
• α: 90°
• β: 92.125 ± 0.004°
• γ: 90°
• Cell volume: 3945.3 ± 1.5 ų
• Cell temperature: 213 ± 2 K
• Ambient diffraction temperature: 213 ± 2 K
• Number of distinct elements: 5
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/n 1
• Hall space group symbol: -P 2yn
• Residual factor for all reflections: 0.0687
• Residual factor for significantly intense reflections: 0.0459
• Weighted residual factors for significantly intense reflections: 0.1221
• Weighted residual factors for all reflections included in the refinement: 0.1351
• Goodness-of-fit parameter for all reflections included in the refinement: 1.065
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No