Information card for entry 7101850

Structure parameters

• Formula: C17.75 H22 As Cl4 Ga N2
• Calculated formula: C17.75 H22 As Cl4 Ga N2
• Title of publication: Diamidonaphthalene-supported pnictogenium cations: synthesis of an N-heterocyclic stibenium cation by a novel protonation route.
• Authors of publication: Spinney, Heather A; Korobkov, Ilia; Richeson, Darrin S
• Journal of publication: Chemical communications (Cambridge, England)
• Year of publication: 2007
• Journal issue: 16
• Pages of publication: 1647 - 1649
• a: 7.233 ± 0.002 Å
• b: 17.314 ± 0.006 Å
• c: 19.58 ± 0.007 Å
• α: 90°
• β: 99.501 ± 0.006°
• γ: 90°
• Cell volume: 2418.3 ± 1.4 ų
• Cell temperature: 198 ± 2 K
• Ambient diffraction temperature: 198 ± 2 K
• Number of distinct elements: 6
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/n 1
• Hall space group symbol: -P 2yn
• Residual factor for all reflections: 0.1085
• Residual factor for significantly intense reflections: 0.0605
• Weighted residual factors for significantly intense reflections: 0.1343
• Weighted residual factors for all reflections included in the refinement: 0.155
• Goodness-of-fit parameter for all reflections included in the refinement: 1.028
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No