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Information card for entry 7101865
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Coordinates | 7101865.cif |
---|---|
Original paper (by DOI) | HTML |
Formula | C24 H56 Cs2 O23 P2 |
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Calculated formula | C24 H50 Cs2 O23 P2 |
Title of publication | Reversible solid-state reaction between 18-Crown[6] and M[H2PO4](M = K, Rb, Cs) and an investigation of the decomplexation process. |
Authors of publication | Braga, Dario; Polito, Marco; Dichiarante, Elena; Rubini, Katia; Grepioni, Fabrizia |
Journal of publication | Chemical communications (Cambridge, England) |
Year of publication | 2007 |
Journal issue | 16 |
Pages of publication | 1594 - 1596 |
a | 25.042 ± 0.005 Å |
b | 8.248 ± 0.003 Å |
c | 20.208 ± 0.003 Å |
α | 90° |
β | 99.66 ± 0.02° |
γ | 90° |
Cell volume | 4114.7 ± 1.8 Å3 |
Cell temperature | 293 ± 2 K |
Ambient diffraction temperature | 293 ± 2 K |
Number of distinct elements | 5 |
Space group number | 15 |
Hermann-Mauguin space group symbol | C 1 2/c 1 |
Hall space group symbol | -C 2yc |
Residual factor for all reflections | 0.0462 |
Residual factor for significantly intense reflections | 0.0354 |
Weighted residual factors for significantly intense reflections | 0.0964 |
Weighted residual factors for all reflections included in the refinement | 0.1032 |
Goodness-of-fit parameter for all reflections included in the refinement | 1.025 |
Diffraction radiation wavelength | 0.71073 Å |
Diffraction radiation type | MoKα |
Has coordinates | Yes |
Has disorder | Yes |
Has Fobs | No |
For the version history of this entry, please navigate to main COD server.
The link is: https://www.crystallography.net/7101865.html
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