Information card for entry 7101879

Structure parameters

• Formula: C12 H54 N9 Ni6 O43 P W9
• Calculated formula: C12 H42 N9 Ni6 O43 P W9
• Title of publication: Combination between lacunary polyoxometalates and high-nuclear transition metal clusters under hydrothermal conditions: I. from isolated cluster to 1-D chain.
• Authors of publication: Zheng, Shou-Tian; Yuan, Da-Qiang; Jia, Hong-Peng; Zhang, Jie; Yang, Guo-Yu
• Journal of publication: Chemical communications (Cambridge, England)
• Year of publication: 2007
• Journal issue: 18
• Pages of publication: 1858 - 1860
• a: 16.4477 ± 0.0003 Å
• b: 19.4046 ± 0.0003 Å
• c: 16.2221 ± 0.0001 Å
• α: 90°
• β: 90°
• γ: 90°
• Cell volume: 5177.46 ± 0.13 ų
• Cell temperature: 274 ± 2 K
• Ambient diffraction temperature: 274 ± 2 K
• Number of distinct elements: 7
• Space group number: 62
• Hermann-Mauguin space group symbol: P n m a
• Hall space group symbol: -P 2ac 2n
• Residual factor for significantly intense reflections: 0.0409
• Weighted residual factors for significantly intense reflections: 0.0826
• Weighted residual factors for all reflections included in the refinement: 0.0864
• Goodness-of-fit parameter for all reflections included in the refinement: 1.188
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No