Information card for entry 7101883

Structure parameters

• Formula: C38 H66 Cl4 O2 Ru2
• Calculated formula: C38 H66 Cl4 O2 Ru2
• Title of publication: A new coupling reaction for the synthesis of ruthenium half-sandwich complexes with sterically demanding cyclopentadienyl ligands.
• Authors of publication: Gauthier, Sébastien; Solari, Euro; Dutta, Barnali; Scopelliti, Rosario; Severin, Kay
• Journal of publication: Chemical communications (Cambridge, England)
• Year of publication: 2007
• Journal issue: 18
• Pages of publication: 1837 - 1839
• a: 23.624 ± 0.002 Å
• b: 14.0305 ± 0.001 Å
• c: 12.2973 ± 0.0008 Å
• α: 90°
• β: 90.572 ± 0.006°
• γ: 90°
• Cell volume: 4075.8 ± 0.5 ų
• Cell temperature: 140 ± 2 K
• Ambient diffraction temperature: 140 ± 2 K
• Number of distinct elements: 5
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/c 1
• Hall space group symbol: -P 2ybc
• Residual factor for all reflections: 0.0823
• Residual factor for significantly intense reflections: 0.0586
• Weighted residual factors for significantly intense reflections: 0.1438
• Weighted residual factors for all reflections included in the refinement: 0.1557
• Goodness-of-fit parameter for all reflections included in the refinement: 0.995
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No