Information card for entry 7102149

Structure parameters

• Formula: C63 H99 N2 P Pb Si2
• Calculated formula: C63 H99 N2 P Pb Si2
• Title of publication: A new type of heteroleptic complex of divalent lead and synthesis of the P-plumbyleniophosphasilene, R2Si=P‒Pb(L): (L = β-diketiminate)
• Authors of publication: Yao, Shenglai; Block, Stefan; Brym, Markus; Driess, Matthias
• Journal of publication: Chemical Communications (Cambridge, United Kingdom)
• Year of publication: 2007
• Journal issue: 37
• Pages of publication: 3844 - 3846
• a: 12.4953 ± 0.0002 Å
• b: 18.9054 ± 0.0003 Å
• c: 14.3412 ± 0.0002 Å
• α: 90°
• β: 109.26 ± 0.0017°
• γ: 90°
• Cell volume: 3198.18 ± 0.08 ų
• Cell temperature: 150 ± 2 K
• Ambient diffraction temperature: 150 ± 2 K
• Number of distinct elements: 6
• Space group number: 11
• Hermann-Mauguin space group symbol: P 1 21/m 1
• Hall space group symbol: -P 2yb
• Residual factor for all reflections: 0.0301
• Residual factor for significantly intense reflections: 0.0219
• Weighted residual factors for significantly intense reflections: 0.0558
• Weighted residual factors for all reflections included in the refinement: 0.0616
• Goodness-of-fit parameter for all reflections included in the refinement: 1.191
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No