Information card for entry 7102168

Structure parameters

• Formula: C85 H36 Ag9 Cl2 N O50 Os13 P2
• Calculated formula: C85 H32 Ag9 Cl2 N O50 Os13 P2
• SMILES: [Os]1([Os]2([Os]3451([Ag]1678([Os]9%10%11%12([Os]([Os]9([Ag]9%13%14%12[Os]%12%15%16%17([Os]([Os]%12(C#[O])(C#[O])(C#[O])C#[O])([Ag]%12%18%19%16[Os]%16%20%21%22([Ag]%23231[Ag]17%109%12%16([Ag]2379%18%20%23([Os]%10%12%16%18([Os]([Os]%10(C#[O])(C#[O])(C#[O])C#[O])([Ag]462%12[Ag]8%11%1313%16[Ag]%14%15%197%18C%17=O)(C#[O])(C#[O])(C#[O])C#[O])(C#[O])(C9=O)C#[O])C%21=O)C%22=O)(C#[O])C#[O])(C#[O])(C#[O])(C#[O])C#[O])(C#[O])C#[O])(C#[O])(C#[O])(C#[O])C#[O])(C#[O])(C#[O])(C#[O])C#[O])(C#[O])(C#[O])C#[O])C5=O)(C#[O])C#[O])(C#[O])(C#[O])(C#[O])C#[O])(C#[O])(C#[O])(C#[O])C#[O].ClCCl.P(=N[P+](c1ccccc1)(c1ccccc1)c1ccccc1)(c1ccccc1)(c1ccccc1)c1ccccc1.O.O
• Title of publication: Synthesis and characterisation of high-nuclearity osmium-silver mixed-metal clusters.
• Authors of publication: Lee, Yui-Bing; Wong, Wing-Tak
• Journal of publication: Chemical communications (Cambridge, England)
• Year of publication: 2007
• Journal issue: 38
• Pages of publication: 3924 - 3926
• a: 19.24 ± 0.003 Å
• b: 19.413 ± 0.003 Å
• c: 19.787 ± 0.003 Å
• α: 99.23 ± 0.003°
• β: 94.512 ± 0.003°
• γ: 109.734 ± 0.003°
• Cell volume: 6795.7 ± 1.8 ų
• Cell temperature: 301 ± 1 K
• Number of distinct elements: 8
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for significantly intense reflections: 0.052
• Weighted residual factors for all reflections included in the refinement: 0.0594
• Goodness-of-fit parameter for all reflections included in the refinement: 1.027
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No