Crystallography Open Database

Information card for entry 7102191

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Coordinates	7102191.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C58 H104 Ge2 O P2
Calculated formula	C58 H104 Ge2 O P2
Title of publication	1,3-Digermacyclobutanes with exocyclic C=P and C=P=S double bonds.
Authors of publication	Petrar, Petronela Maria; Nemes, Gabriela; Silaghi-Dumitrescu, Ioan; Ranaivonjatovo, Henri; Gornitzka, Heinz; Escudié, Jean
Journal of publication	Chemical communications (Cambridge, England)
Year of publication	2007
Journal issue	40
Pages of publication	4149 - 4151
a	35.416 ± 0.002 Å
b	10.6099 ± 0.0007 Å
c	16.2868 ± 0.0011 Å
α	90°
β	101.109 ± 0.001°
γ	90°
Cell volume	6005.3 ± 0.7 Å³
Cell temperature	173 ± 2 K
Ambient diffraction temperature	173 ± 2 K
Number of distinct elements	5
Space group number	15
Hermann-Mauguin space group symbol	C 1 2/c 1
Hall space group symbol	-C 2yc
Residual factor for all reflections	0.0726
Residual factor for significantly intense reflections	0.0386
Weighted residual factors for significantly intense reflections	0.0748
Weighted residual factors for all reflections included in the refinement	0.0847
Goodness-of-fit parameter for all reflections included in the refinement	0.997
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

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