Information card for entry 7102213

Structure parameters

• Formula: C104.5 H87 Ag6 Cl7 F1.5 Fe3 I5 O0.5 P6.5
• Calculated formula: C104.5 H87 Ag6 Cl7 F1.5 Fe3 I5 O0.5 P6.25
• Title of publication: General formation of trigonal-prismatic [Ag~6~X~5~(dppf)~3~]^+^ (X = Cl, Br, I) through an unusual ligand migration from NiX2(dppf) to AgOTf
• Authors of publication: Teo, Peili; Koh, Lip Lin; Hor, T. S. Andy
• Journal of publication: Chemical Communications (Cambridge, United Kingdom)
• Year of publication: 2007
• Journal issue: 41
• Pages of publication: 4221 - 4223
• a: 14.0043 ± 0.0014 Å
• b: 14.5664 ± 0.0015 Å
• c: 28.009 ± 0.003 Å
• α: 80.22 ± 0.002°
• β: 89.298 ± 0.002°
• γ: 78.533 ± 0.002°
• Cell volume: 5516.8 ± 1 ų
• Cell temperature: 223 ± 2 K
• Ambient diffraction temperature: 223 ± 2 K
• Number of distinct elements: 9
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.1684
• Residual factor for significantly intense reflections: 0.1484
• Weighted residual factors for significantly intense reflections: 0.3204
• Weighted residual factors for all reflections included in the refinement: 0.3292
• Goodness-of-fit parameter for all reflections included in the refinement: 1.201
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No