Information card for entry 7102216

Structure parameters

• Formula: C94 H90 Ag3 Cl9 P7
• Calculated formula: C94 H90 Ag3 Cl9 P7
• Title of publication: General formation of trigonal-prismatic [Ag~6~X~5~(dppf)~3~]^+^ (X = Cl, Br, I) through an unusual ligand migration from NiX2(dppf) to AgOTf
• Authors of publication: Teo, Peili; Koh, Lip Lin; Hor, T. S. Andy
• Journal of publication: Chemical Communications (Cambridge, United Kingdom)
• Year of publication: 2007
• Journal issue: 41
• Pages of publication: 4221 - 4223
• a: 14.6609 ± 0.0012 Å
• b: 17.102 ± 0.0014 Å
• c: 19.2916 ± 0.0015 Å
• α: 100.8 ± 0.002°
• β: 92.932 ± 0.002°
• γ: 93.317 ± 0.002°
• Cell volume: 4733.9 ± 0.7 ų
• Cell temperature: 223 ± 2 K
• Ambient diffraction temperature: 223 ± 2 K
• Number of distinct elements: 5
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.1972
• Residual factor for significantly intense reflections: 0.1148
• Weighted residual factors for significantly intense reflections: 0.2202
• Weighted residual factors for all reflections included in the refinement: 0.2556
• Goodness-of-fit parameter for all reflections included in the refinement: 1.093
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No