Information card for entry 7102283

Structure parameters

• Formula: C59.5 H142 N6 P4 Si4 Ti2
• Calculated formula: C59.5 H124 N6 P4 Si4 Ti2
• Title of publication: Transition metal dinitrogen complexes supported by a versatile monoanionic [N2P2] ligand.
• Authors of publication: Chomitz, Wayne A; Arnold, John
• Journal of publication: Chemical communications (Cambridge, England)
• Year of publication: 2007
• Journal issue: 45
• Pages of publication: 4797 - 4799
• a: 19.224 ± 0.004 Å
• b: 18.899 ± 0.004 Å
• c: 23.297 ± 0.005 Å
• α: 90°
• β: 109.599 ± 0.002°
• γ: 90°
• Cell volume: 7974 ± 3 ų
• Cell temperature: 148 ± 2 K
• Ambient diffraction temperature: 148 ± 2 K
• Number of distinct elements: 6
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/c 1
• Hall space group symbol: -P 2ybc
• Residual factor for all reflections: 0.1506
• Residual factor for significantly intense reflections: 0.0578
• Weighted residual factors for significantly intense reflections: 0.1176
• Weighted residual factors for all reflections included in the refinement: 0.1431
• Goodness-of-fit parameter for all reflections included in the refinement: 0.981
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No