Information card for entry 7102289

Structure parameters

• Formula: C63 H96 N4 O28 Pd8
• Calculated formula: C63 H96 N4 O28 Pd8
• Title of publication: NO-disproportionation, promoted by Pd-cluster: formation and X-ray structure of Pd8(micro-CO)4(micro-OOCCMe3)8[micro-N(=O)O-]4.
• Authors of publication: Stromnova, Tatiana A; Shishilov, Oleg N; Churakov, Andrei V; Kuz'mina, Lyudmila G; Howard, Judith A K
• Journal of publication: Chemical communications (Cambridge, England)
• Year of publication: 2007
• Journal issue: 45
• Pages of publication: 4800 - 4802
• a: 20.2125 ± 0.0013 Å
• b: 19.3904 ± 0.0013 Å
• c: 23.8068 ± 0.0016 Å
• α: 90°
• β: 114.518 ± 0.001°
• γ: 90°
• Cell volume: 8489.2 ± 1 ų
• Cell temperature: 115 ± 2 K
• Ambient diffraction temperature: 115 ± 2 K
• Number of distinct elements: 5
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/n 1
• Hall space group symbol: -P 2yn
• Residual factor for all reflections: 0.0814
• Residual factor for significantly intense reflections: 0.0513
• Weighted residual factors for significantly intense reflections: 0.127
• Weighted residual factors for all reflections included in the refinement: 0.1394
• Goodness-of-fit parameter for all reflections included in the refinement: 1.01
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No