Information card for entry 7102299

Structure parameters

• Common name: 1
• Formula: C66 H88 Sn7
• Calculated formula: C66 H88 Sn7
• Title of publication: Convergent syntheses of [Sn7{C6H3-2,6-(C6H3-2,6-iPr2)2}2]: a cluster with a rare pentagonal bipyramidal motif
• Authors of publication: Rivard, Eric; Steiner, Jochen; Fettinger, James C.; Giuliani, Jason R.; Augustine, Matthew P.; Power, Philip P.
• Journal of publication: Chemical Communications (Cambridge, United Kingdom)
• Year of publication: 2007
• Journal issue: 46
• Pages of publication: 4919 - 4921
• a: 15.6747 ± 0.0005 Å
• b: 17.1734 ± 0.0005 Å
• c: 24.6446 ± 0.0007 Å
• α: 90°
• β: 99.012 ± 0.001°
• γ: 90°
• Cell volume: 6552.1 ± 0.3 ų
• Cell temperature: 90 ± 2 K
• Ambient diffraction temperature: 90 ± 2 K
• Number of distinct elements: 3
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/c 1
• Hall space group symbol: -P 2ybc
• Residual factor for all reflections: 0.0433
• Residual factor for significantly intense reflections: 0.034
• Weighted residual factors for significantly intense reflections: 0.0856
• Weighted residual factors for all reflections included in the refinement: 0.0892
• Goodness-of-fit parameter for all reflections included in the refinement: 1.081
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No