Information card for entry 7102354

Structure parameters

• Formula: C116 H134 Cl6 N26 O14 V8
• Calculated formula: C116 H134 Cl6 N26 O14 V8
• Title of publication: Large spin, magnetically anisotropic, octametallic vanadium(iii) clusters with strong ferromagnetic coupling.
• Authors of publication: Shaw, Rachel; Tuna, Floriana; Wernsdorfer, Wolfgang; Barra, Anne-Laure; Collison, David; McInnes, Eric J L
• Journal of publication: Chemical communications (Cambridge, England)
• Year of publication: 2007
• Journal issue: 48
• Pages of publication: 5161 - 5163
• a: 13.2856 ± 0.0008 Å
• b: 14.7996 ± 0.0007 Å
• c: 18.4967 ± 0.0009 Å
• α: 66.701 ± 0.005°
• β: 77.315 ± 0.005°
• γ: 80.523 ± 0.005°
• Cell volume: 3246.4 ± 0.3 ų
• Cell temperature: 100 ± 2 K
• Ambient diffraction temperature: 100 ± 2 K
• Number of distinct elements: 6
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.1141
• Residual factor for significantly intense reflections: 0.0778
• Weighted residual factors for significantly intense reflections: 0.2254
• Weighted residual factors for all reflections included in the refinement: 0.2469
• Goodness-of-fit parameter for all reflections included in the refinement: 0.999
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No