Information card for entry 7102652

Structure parameters

• Formula: C40 H48 O P Pd
• Calculated formula: C40 H48 O P Pd
• Title of publication: Synthesis of two novel dinuclear palladium(I) complexes and studies of their catalytic activity in amination reactions.
• Authors of publication: Christmann, Ute; Vilar, Ramón; White, Andrew J P; Williams, David J
• Journal of publication: Chemical communications (Cambridge, England)
• Year of publication: 2004
• Journal issue: 11
• Pages of publication: 1294 - 1295
• a: 18.999 ± 0.003 Å
• b: 9.953 ± 0.0018 Å
• c: 19.111 ± 0.006 Å
• α: 90°
• β: 102.658 ± 0.016°
• γ: 90°
• Cell volume: 3526 ± 1.3 ų
• Cell temperature: 203 ± 2 K
• Ambient diffraction temperature: 203 ± 2 K
• Number of distinct elements: 5
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/c 1
• Hall space group symbol: -P 2ybc
• Residual factor for all reflections: 0.1187
• Residual factor for significantly intense reflections: 0.0627
• Weighted residual factors for significantly intense reflections: 0.119
• Weighted residual factors for all reflections included in the refinement: 0.1334
• Goodness-of-fit parameter for all reflections included in the refinement: 0.969
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No