Information card for entry 7102654

Structure parameters

• Formula: C20 H27 Cl2 P Pd2
• Calculated formula: C20 H27 Cl2 P Pd2
• SMILES: [Pd]12345[Pd]67([Cl]1)(Cl)[cH]1[cH]4[c]3([cH]5[cH]7[cH]61)c1ccccc1[P]2(C(C)(C)C)C(C)(C)C
• Title of publication: Synthesis of two novel dinuclear palladium(I) complexes and studies of their catalytic activity in amination reactions.
• Authors of publication: Christmann, Ute; Vilar, Ramón; White, Andrew J P; Williams, David J
• Journal of publication: Chemical communications (Cambridge, England)
• Year of publication: 2004
• Journal issue: 11
• Pages of publication: 1294 - 1295
• a: 9.276 ± 0.002 Å
• b: 15.907 ± 0.009 Å
• c: 15.125 ± 0.004 Å
• α: 90°
• β: 102.823 ± 0.019°
• γ: 90°
• Cell volume: 2176.1 ± 1.5 ų
• Cell temperature: 293 ± 2 K
• Ambient diffraction temperature: 293 ± 2 K
• Number of distinct elements: 5
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/n 1
• Hall space group symbol: -P 2yn
• Residual factor for all reflections: 0.0782
• Residual factor for significantly intense reflections: 0.059
• Weighted residual factors for significantly intense reflections: 0.1469
• Weighted residual factors for all reflections included in the refinement: 0.1564
• Goodness-of-fit parameter for all reflections included in the refinement: 1.02
• Diffraction radiation wavelength: 1.54178 Å
• Diffraction radiation type: CuKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No