Information card for entry 7102701

Structure parameters

• Formula: C30 H45 Lu N2 O2 Si2
• Calculated formula: C30 H30 Lu N2 O2 Si2
• Title of publication: C-H activation of a 2,2[prime or minute]-bipyridine ligand within (mono)pentamethylcyclopentadienyl lutetium complexes.
• Authors of publication: Cameron, Thomas M; Gordon, John C; Scott, Brian L; Tumas, William
• Journal of publication: Chemical communications (Cambridge, England)
• Year of publication: 2004
• Journal issue: 12
• Pages of publication: 1398 - 1399
• a: 11.367 ± 0.002 Å
• b: 20.14 ± 0.005 Å
• c: 14.186 ± 0.003 Å
• α: 90°
• β: 98.178 ± 0.004°
• γ: 90°
• Cell volume: 3214.6 ± 1.2 ų
• Cell temperature: 203 ± 2 K
• Ambient diffraction temperature: 203 ± 2 K
• Number of distinct elements: 6
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/n 1
• Hall space group symbol: -P 2yn
• Residual factor for all reflections: 0.1409
• Residual factor for significantly intense reflections: 0.0711
• Weighted residual factors for significantly intense reflections: 0.1155
• Weighted residual factors for all reflections included in the refinement: 0.1315
• Goodness-of-fit parameter for all reflections included in the refinement: 1.256
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No