Information card for entry 7102715

Structure parameters

• Formula: C34 H50 Cl O5 Sb
• Calculated formula: C34 H42 Cl O5 Sb
• Title of publication: Synthesis and X-ray crystal structures of the first antimony and bismuth calixarene complexes.
• Authors of publication: Liu, Lihua; Zakharov, Lev N; Rheingold, Arnold L; Hanna, Tracy A
• Journal of publication: Chemical communications (Cambridge, England)
• Year of publication: 2004
• Journal issue: 13
• Pages of publication: 1472 - 1473
• a: 10.732 ± 0.001 Å
• b: 11.6398 ± 0.0011 Å
• c: 13.985 ± 0.0013 Å
• α: 87.294 ± 0.002°
• β: 72.496 ± 0.001°
• γ: 83.252 ± 0.001°
• Cell volume: 1654.4 ± 0.3 ų
• Cell temperature: 100 ± 2 K
• Ambient diffraction temperature: 100 ± 2 K
• Number of distinct elements: 5
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0368
• Residual factor for significantly intense reflections: 0.0341
• Weighted residual factors for significantly intense reflections: 0.0908
• Weighted residual factors for all reflections included in the refinement: 0.0928
• Goodness-of-fit parameter for all reflections included in the refinement: 1.019
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No