Information card for entry 7102722

Structure parameters

• Formula: C72 H50 F24 N12 O P4 Ru2
• Calculated formula: C72 H48 F24 N12 O P4 Ru2
• Title of publication: Formation of racemic crystals of transition metal complexes by grinding 1 : 1 mixtures of enantiomeric crystals.
• Authors of publication: Nakamura, Asao; Sato, Tomohiro; Kuroda, Reiko
• Journal of publication: Chemical communications (Cambridge, England)
• Year of publication: 2004
• Journal issue: 24
• Pages of publication: 2858 - 2859
• a: 36.81 ± 0.003 Å
• b: 15.7955 ± 0.0012 Å
• c: 12.1174 ± 0.0009 Å
• α: 90°
• β: 101.681 ± 0.001°
• γ: 90°
• Cell volume: 6899.6 ± 0.9 ų
• Cell temperature: 100 ± 2 K
• Ambient diffraction temperature: 100 ± 2 K
• Number of distinct elements: 7
• Space group number: 9
• Hermann-Mauguin space group symbol: C 1 c 1
• Hall space group symbol: C -2yc
• Residual factor for all reflections: 0.0348
• Residual factor for significantly intense reflections: 0.0347
• Weighted residual factors for significantly intense reflections: 0.0849
• Weighted residual factors for all reflections included in the refinement: 0.0849
• Goodness-of-fit parameter for all reflections included in the refinement: 1.158
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No