Information card for entry 7102724

Structure parameters

• Formula: C72 H50 F24 N12 O Os2 P4
• Calculated formula: C72 H48 F24 N12 O Os2 P4
• Title of publication: Formation of racemic crystals of transition metal complexes by grinding 1 : 1 mixtures of enantiomeric crystals.
• Authors of publication: Nakamura, Asao; Sato, Tomohiro; Kuroda, Reiko
• Journal of publication: Chemical communications (Cambridge, England)
• Year of publication: 2004
• Journal issue: 24
• Pages of publication: 2858 - 2859
• a: 36.6813 ± 0.0019 Å
• b: 15.839 ± 0.0008 Å
• c: 12.1451 ± 0.0006 Å
• α: 90°
• β: 101.665 ± 0.001°
• γ: 90°
• Cell volume: 6910.5 ± 0.6 ų
• Cell temperature: 100 ± 2 K
• Ambient diffraction temperature: 100 ± 2 K
• Number of distinct elements: 7
• Space group number: 9
• Hermann-Mauguin space group symbol: C 1 c 1
• Hall space group symbol: C -2yc
• Residual factor for all reflections: 0.0321
• Residual factor for significantly intense reflections: 0.0313
• Weighted residual factors for significantly intense reflections: 0.0756
• Weighted residual factors for all reflections included in the refinement: 0.0766
• Goodness-of-fit parameter for all reflections included in the refinement: 1.032
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No