Information card for entry 7102767

Structure parameters

• Formula: C244 H190 Cl4 Co16 N8 O32 P16 S4
• Calculated formula: C244 H190 Cl4 Co16 N8 O32 P16 S4
• Title of publication: Assembling metals and clusters around an octaphosphine ligand based on N-substituted bis(diphenylphosphanyl)amines: structural characterization of dendrimer-like Co~12~ and Co~16~ branched clusters
• Authors of publication: Rodriguez-Zubiri, Mireia; Gallo, Vito; Rosé, Jacky; Welter, Richard; Braunstein, Pierre
• Journal of publication: Chemical Communications (Cambridge, United Kingdom)
• Year of publication: 2008
• Journal issue: 1
• Pages of publication: 64 - 66
• a: 18.73 ± 0.0004 Å
• b: 19.79 ± 0.0004 Å
• c: 20.42 ± 0.0007 Å
• α: 98.62 ± 0.0009°
• β: 97.845 ± 0.0009°
• γ: 116.426 ± 0.0015°
• Cell volume: 6522.7 ± 0.3 ų
• Cell temperature: 173 ± 2 K
• Ambient diffraction temperature: 173 ± 2 K
• Number of distinct elements: 8
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.3234
• Residual factor for significantly intense reflections: 0.1615
• Weighted residual factors for significantly intense reflections: 0.2633
• Weighted residual factors for all reflections included in the refinement: 0.3302
• Goodness-of-fit parameter for all reflections included in the refinement: 1.229
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No