Information card for entry 7102802

Structure parameters

• Formula: C22 H53 N4 Na Zn
• Calculated formula: C22 H53 N4 Na Zn
• SMILES: C1[N](C)(C)[Na]2([N]([Zn]([N]2(C(C)C)C(C)C)C(C)(C)C)(C(C)C)C(C)C)[N](C)(C)C1
• Title of publication: Transamination chemistry of sodium TMP-zincate: synthesis and crystal structure of a chiral amidozincate
• Authors of publication: Armstrong, David R.; Clegg, William; Dale, Sophie H.; García-Álvarez, Joaquín; Harrington, Ross W.; Hevia, Eva; Honeyman, Gordon W.; Kennedy, Alan R.; Mulvey, Robert E.; O'Hara, Charles T.
• Journal of publication: Chemical Communications (Cambridge, United Kingdom)
• Year of publication: 2008
• Journal issue: 2
• Pages of publication: 187 - 189
• a: 10.8591 ± 0.0009 Å
• b: 18.6245 ± 0.0016 Å
• c: 14.1986 ± 0.0012 Å
• α: 90°
• β: 100.566 ± 0.0013°
• γ: 90°
• Cell volume: 2822.9 ± 0.4 ų
• Cell temperature: 150 ± 2 K
• Ambient diffraction temperature: 150 ± 2 K
• Number of distinct elements: 5
• Space group number: 15
• Hermann-Mauguin space group symbol: C 1 2/c 1
• Hall space group symbol: -C 2yc
• Residual factor for all reflections: 0.0548
• Residual factor for significantly intense reflections: 0.053
• Weighted residual factors for significantly intense reflections: 0.123
• Weighted residual factors for all reflections included in the refinement: 0.1239
• Goodness-of-fit parameter for all reflections included in the refinement: 1.229
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No