Crystallography Open Database

Information card for entry 7102842

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Coordinates	7102842.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C78 H111 N O Pd4
Calculated formula	C78 H93 N O Pd4
Title of publication	A stable zerovalent palladium chain enveloped by a pi-electron sheath of conjugated polyene ligands.
Authors of publication	Tatsumi, Yasuki; Murahashi, Tetsuro; Okada, Mitsue; Ogoshi, Sensuke; Kurosawa, Hideo
Journal of publication	Chemical communications (Cambridge, England)
Year of publication	2008
Journal issue	4
Pages of publication	477 - 479
a	13.826 ± 0.0005 Å
b	15.3256 ± 0.0005 Å
c	18.6303 ± 0.0005 Å
α	71.357 ± 0.0008°
β	83.123 ± 0.0009°
γ	71.549 ± 0.0009°
Cell volume	3547.44 ± 0.19 Å³
Cell temperature	123.1 K
Number of distinct elements	5
Space group number	2
Hermann-Mauguin space group symbol	P -1
Hall space group symbol	-P 1
Residual factor for significantly intense reflections	0.0987
Weighted residual factors for all reflections included in the refinement	0.3055
Goodness-of-fit parameter for all reflections included in the refinement	1.03
Diffraction radiation wavelength	0.71075 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

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