Information card for entry 7102876

Structure parameters

• Common name: tetra(N,N'-diphenyl-isonicotamidate) dirhodium, dimethylsulfoxide pentasolvate, dihydrate
• Chemical name: tetra(N,N'-diphenyl-isonicotamidate) dirhodium, dimethylsulfoxide pentasolvate, dihydrate
• Formula: C77 H73 N12 O3.5 Rh2 S2.5
• Calculated formula: C76.999 H72.997 N12 O3.4995 Rh2 S2.4995
• Title of publication: Facile synthesis of multinuclear complexes based on a tetra(4-pyridyl)amidinate dirhodium(II) dimer
• Authors of publication: Chartrand, Daniel; Hanan, Garry S.
• Journal of publication: Chemical Communications (Cambridge, United Kingdom)
• Year of publication: 2008
• Journal issue: 6
• Pages of publication: 727 - 729
• a: 25.6654 ± 0.0014 Å
• b: 27.3601 ± 0.0015 Å
• c: 21.9392 ± 0.0011 Å
• α: 90°
• β: 113.913 ± 0.003°
• γ: 90°
• Cell volume: 14083.4 ± 1.3 ų
• Cell temperature: 100 ± 2 K
• Ambient diffraction temperature: 100 ± 2 K
• Number of distinct elements: 6
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/c 1
• Hall space group symbol: -P 2ybc
• Residual factor for all reflections: 0.0577
• Residual factor for significantly intense reflections: 0.0535
• Weighted residual factors for significantly intense reflections: 0.152
• Weighted residual factors for all reflections included in the refinement: 0.1548
• Goodness-of-fit parameter for all reflections included in the refinement: 1.072
• Diffraction radiation wavelength: 1.54178 Å
• Diffraction radiation type: CuKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No