Information card for entry 7102887

Structure parameters

• Formula: C75.5 H59 Cl3 F12 N2 P2 Pd Sb2
• Calculated formula: C75.5 H59 Cl3 F12 N2 P2 Pd Sb2
• Title of publication: Stereoselective coordination of ditopic phospholyl-azahelicenes: a novel approach towards structural diversity in chiral pi-conjugated assemblies.
• Authors of publication: Shen, Wenting; Graule, Sébastien; Crassous, Jeanne; Lescop, Christophe; Gornitzka, Heinz; Réau, Régis
• Journal of publication: Chemical communications (Cambridge, England)
• Year of publication: 2008
• Journal issue: 7
• Pages of publication: 850 - 852
• a: 18.695 ± 0.005 Å
• b: 18.695 ± 0.005 Å
• c: 81.28 ± 0.002 Å
• α: 90°
• β: 90°
• γ: 90°
• Cell volume: 28408 ± 11 ų
• Cell temperature: 100 ± 2 K
• Ambient diffraction temperature: 100 ± 2 K
• Number of distinct elements: 8
• Space group number: 88
• Hermann-Mauguin space group symbol: I 41/a :2
• Hall space group symbol: -I 4ad
• Residual factor for all reflections: 0.1827
• Residual factor for significantly intense reflections: 0.1074
• Weighted residual factors for significantly intense reflections: 0.2213
• Weighted residual factors for all reflections included in the refinement: 0.2542
• Goodness-of-fit parameter for all reflections included in the refinement: 1.128
• Diffraction radiation wavelength: 0.71069 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No