1,2-Diphosphinobenzene as a synthon for the 1,2,3-triphospha- and 2-arsa-1,3-diphosphaindenyl anions and a stable organo derivative of the P8 unit of Hittorf's phosphorus.
Authors of publication
Butts, Craig P; Green, Michael; Hooper, Thomas N; Kilby, Richard J; McGrady, John E; Pantazis, Dimitrios A; Russell, Christopher A
Journal of publication
Chemical communications (Cambridge, England)
Year of publication
2008
Journal issue
7
Pages of publication
856 - 858
a
6.6704 ± 0.0001 Å
b
10.8568 ± 0.0002 Å
c
10.9239 ± 0.0002 Å
α
92.7378 ± 0.0011°
β
92.6832 ± 0.0012°
γ
107.17 ± 0.0011°
Cell volume
753.44 ± 0.02 Å3
Cell temperature
100 ± 2 K
Ambient diffraction temperature
100 K
Number of distinct elements
3
Space group number
2
Hermann-Mauguin space group symbol
P -1
Hall space group symbol
-P 1
Residual factor for all reflections
0.0404
Residual factor for significantly intense reflections
0.0372
Weighted residual factors for significantly intense reflections
0.0999
Weighted residual factors for all reflections included in the refinement
0.1028
Goodness-of-fit parameter for all reflections included in the refinement
