Information card for entry 7103107

Structure parameters

• Formula: C180 H250 Cl8 N8 O13 Zr4
• Calculated formula: C180 H250 Cl8 N8 O13 Zr4
• Title of publication: Construction of C1-symmetric zirconium complexes by the design of new Salan ligands. Coordination chemistry and preliminary polymerisation catalysis studies.
• Authors of publication: Cohen, Ad; Yeori, Adi; Kopilov, Jacob; Goldberg, Israel; Kol, Moshe
• Journal of publication: Chemical communications (Cambridge, England)
• Year of publication: 2008
• Journal issue: 18
• Pages of publication: 2149 - 2151
• a: 28.4938 ± 0.0006 Å
• b: 17.8978 ± 0.0003 Å
• c: 17.8233 ± 0.0003 Å
• α: 90°
• β: 90°
• γ: 90°
• Cell volume: 9089.5 ± 0.3 ų
• Cell temperature: 110 ± 2 K
• Ambient diffraction temperature: 110 ± 2 K
• Number of distinct elements: 6
• Space group number: 45
• Hermann-Mauguin space group symbol: I b a 2
• Hall space group symbol: I 2 -2c
• Residual factor for all reflections: 0.08
• Residual factor for significantly intense reflections: 0.051
• Weighted residual factors for significantly intense reflections: 0.1136
• Weighted residual factors for all reflections included in the refinement: 0.1247
• Goodness-of-fit parameter for all reflections included in the refinement: 1.027
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No