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Information card for entry 7103126
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Coordinates | 7103126.cif |
---|---|
Original paper (by DOI) | HTML |
Formula | C35 H33 N3 O4 |
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Calculated formula | C35 H33 N3 O4 |
Title of publication | Direct synthesis of bicyclic guanidines through unprecedented palladium(ii) catalysed diamination with copper chloride as oxidant. |
Authors of publication | Hövelmann, Claas H; Streuff, Jan; Brelot, Lydia; Muñiz, Kilian |
Journal of publication | Chemical communications (Cambridge, England) |
Year of publication | 2008 |
Journal issue | 20 |
Pages of publication | 2334 - 2336 |
a | 9.963 ± 0.0005 Å |
b | 10.062 ± 0.0005 Å |
c | 15.785 ± 0.0005 Å |
α | 89.717 ± 0.003° |
β | 76.596 ± 0.003° |
γ | 67.802 ± 0.002° |
Cell volume | 1419.21 ± 0.11 Å3 |
Cell temperature | 173 ± 2 K |
Ambient diffraction temperature | 173 ± 2 K |
Number of distinct elements | 4 |
Space group number | 2 |
Hermann-Mauguin space group symbol | P -1 |
Hall space group symbol | -P 1 |
Residual factor for all reflections | 0.0755 |
Residual factor for significantly intense reflections | 0.048 |
Weighted residual factors for significantly intense reflections | 0.1162 |
Weighted residual factors for all reflections included in the refinement | 0.13 |
Goodness-of-fit parameter for all reflections included in the refinement | 1.05 |
Diffraction radiation wavelength | 0.71073 Å |
Diffraction radiation type | MoKα |
Has coordinates | Yes |
Has disorder | Yes |
Has Fobs | No |
For the version history of this entry, please navigate to main COD server.
The link is: https://www.crystallography.net/7103126.html
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