Information card for entry 7103312

Structure parameters

• Formula: C70.5 H86 Al2 I2 N4
• Calculated formula: C70.5 H86 Al2 I2 N4
• Title of publication: Synthesis and reactivity of bis-pentamethylcyclopentadienyl diiododialane (Cp*AlI)2: an aluminium(II) precursor to (Cp*Al)4.
• Authors of publication: Minasian, Stefan G; Arnold, John
• Journal of publication: Chemical communications (Cambridge, England)
• Year of publication: 2008
• Journal issue: 34
• Pages of publication: 4043 - 4045
• a: 10.6194 ± 0.001 Å
• b: 15.9477 ± 0.0015 Å
• c: 21.317 ± 0.002 Å
• α: 105.315 ± 0.002°
• β: 94.491 ± 0.002°
• γ: 102.408 ± 0.001°
• Cell volume: 3365.5 ± 0.5 ų
• Cell temperature: 150 ± 2 K
• Ambient diffraction temperature: 150 ± 2 K
• Number of distinct elements: 5
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0868
• Residual factor for significantly intense reflections: 0.0563
• Weighted residual factors for significantly intense reflections: 0.133
• Weighted residual factors for all reflections included in the refinement: 0.1503
• Goodness-of-fit parameter for all reflections included in the refinement: 1.033
• Diffraction radiation wavelength: 0.7749 Å
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No