Information card for entry 7103494

Structure parameters

• Common name: (1,4,8,11- tetrathiacyclotetradecane)bis(dichlorogermanium(ii)) dichloromethane solvate
• Chemical name: (1,4,8,11-tetrathiacyclotetradecane)bis(dichlorogermanium(II)) dichloromethane solvate
• Formula: C10.7 H21.41 Cl5.41 Ge2 S4
• Calculated formula: C10.701 H21.4 Cl5.401 Ge2 S4
• Title of publication: Coordination networks derived from germanium(ii) thioether macrocyclic complexes-the first authenticated chalcogenoether complexes of Ge(ii).
• Authors of publication: Cheng, Fei; Hector, Andrew L; Levason, William; Reid, Gillian; Webster, Michael; Zhang, Wenjian
• Journal of publication: Chemical communications (Cambridge, England)
• Year of publication: 2008
• Journal issue: 43
• Pages of publication: 5508 - 5510
• a: 4.9051 ± 0.001 Å
• b: 22.596 ± 0.003 Å
• c: 20.973 ± 0.003 Å
• α: 90°
• β: 90°
• γ: 90°
• Cell volume: 2324.5 ± 0.7 ų
• Cell temperature: 120 ± 2 K
• Ambient diffraction temperature: 120 ± 2 K
• Number of distinct elements: 5
• Space group number: 57
• Hermann-Mauguin space group symbol: P b c m
• Hall space group symbol: -P 2c 2b
• Residual factor for all reflections: 0.0876
• Residual factor for significantly intense reflections: 0.0631
• Weighted residual factors for significantly intense reflections: 0.1405
• Weighted residual factors for all reflections included in the refinement: 0.1572
• Goodness-of-fit parameter for all reflections included in the refinement: 1.076
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No