Azaarene cis-dihydrodiol-derived 2,2'-bipyridine ligands for asymmetric allylic oxidation and cyclopropanation.
Authors of publication
Boyd, Derek R; Sharma, Narain D; Sbircea, Lenuta; Murphy, Deirdre; Belhocine, Tayeb; Malone, John F; James, Stuart L; Allen, Christopher C R; Hamilton, John T G
Journal of publication
Chemical communications (Cambridge, England)
Year of publication
2008
Journal issue
43
Pages of publication
5535 - 5537
a
10.113 ± 0.005 Å
b
7.73 ± 0.004 Å
c
13.915 ± 0.007 Å
α
90°
β
93.646 ± 0.008°
γ
90°
Cell volume
1085.6 ± 0.9 Å3
Cell temperature
293 ± 2 K
Ambient diffraction temperature
293 ± 2 K
Number of distinct elements
4
Space group number
4
Hermann-Mauguin space group symbol
P 1 21 1
Hall space group symbol
P 2yb
Residual factor for all reflections
0.08
Residual factor for significantly intense reflections
0.0449
Weighted residual factors for significantly intense reflections
0.1042
Weighted residual factors for all reflections included in the refinement
0.1321
Goodness-of-fit parameter for all reflections included in the refinement