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Information card for entry 7103936
Preview
Coordinates | 7103936.cif |
---|---|
Original paper (by DOI) | HTML |
Formula | C39 H38 Ge N2 O8 P2 Si2 W2 |
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Calculated formula | C39 H38 Ge N2 O8 P2 Si2 W2 |
SMILES | [W]([Ge]12[W]3([N]([Si](C)(C)C)=P([C@]13P(=[N]2[Si](C)(C)C)(c1ccccc1)c1ccccc1)(c1ccccc1)c1ccccc1)(C#[O])(C#[O])C#[O])(C#[O])(C#[O])(C#[O])(C#[O])C#[O] |
Title of publication | A novel synthesis of metallogermacyclopropane and molybdenum bis(iminophosphorano)carbene complexes from bisgermavinylidene |
Authors of publication | Leung, Wing-Por; So, Cheuk-Wai; Wang, Jin-Zhi; Mak, Thomas C. W. |
Journal of publication | Chemical Communications (Cambridge, United Kingdom) |
Year of publication | 2003 |
Journal issue | 2 |
Pages of publication | 248 - 249 |
a | 10.9208 ± 0.0015 Å |
b | 19.945 ± 0.003 Å |
c | 20.951 ± 0.003 Å |
α | 90° |
β | 90° |
γ | 90° |
Cell volume | 4563.3 ± 1.1 Å3 |
Cell temperature | 294 ± 2 K |
Ambient diffraction temperature | 294 ± 2 K |
Number of distinct elements | 8 |
Space group number | 19 |
Hermann-Mauguin space group symbol | P 21 21 21 |
Hall space group symbol | P 2ac 2ab |
Residual factor for all reflections | 0.037 |
Residual factor for significantly intense reflections | 0.0277 |
Weighted residual factors for significantly intense reflections | 0.0628 |
Weighted residual factors for all reflections included in the refinement | 0.0836 |
Goodness-of-fit parameter for all reflections included in the refinement | 1.09 |
Diffraction radiation wavelength | 0.71073 Å |
Diffraction radiation type | MoKα |
Has coordinates | Yes |
Has disorder | No |
Has Fobs | No |
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The link is: https://www.crystallography.net/7103936.html
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