Information card for entry 7103944
Formula
C8 H10 Cl3 N O
Calculated formula
C8 H10 Cl3 N O
SMILES
ClC1(Cl)[C@H]([C@H]2N(CCC2)C1=O)CCl
Title of publication
Organoruthenium(II) and (III) amidinates, (η5-C5Me5)Ru(η-amidinate) and (η5-C5Me5)RuCl(η-amidinate), as unique redox catalysts for the intramolecular Kharasch reactions: Facile access to a pyrrolizidine alkaloid skeleton under mild conditions
Authors of publication
Nagashima, Hideo; Gondo, Mitsuru; Masuda, Satoshi; Kondo, Hideo; Yamaguchi, Yoshitaka; Matsubara, Kouki
Journal of publication
Chemical Communications (Cambridge, United Kingdom)
Year of publication
2003
Journal issue
3
Pages of publication
442 - 443
a
9.3085 ± 0.0006 Å
b
15.0641 ± 0.001 Å
c
7.4597 ± 0.0004 Å
α
90°
β
90°
γ
90°
Cell volume
1046.03 ± 0.11 Å3
Cell temperature
293 ± 2 K
Ambient diffraction temperature
293 ± 2 K
Number of distinct elements
5
Space group number
19
Hermann-Mauguin space group symbol
P 21 21 21
Hall space group symbol
P 2ac 2ab
Residual factor for all reflections
0.0463
Residual factor for significantly intense reflections
0.0333
Weighted residual factors for significantly intense reflections
0.0685
Weighted residual factors for all reflections included in the refinement
0.0741
Goodness-of-fit parameter for all reflections included in the refinement
0.966
Diffraction radiation wavelength
0.71069 Å
Diffraction radiation type
MoKα
Has coordinates
Yes
Has disorder
No
Has Fobs
No
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