Information card for entry 7104003

Structure parameters

• Formula: C40 H65 Li2 N7 Si2
• Calculated formula: C40.005 H65 Li2 N7 Si2
• Title of publication: An N-lithio-indole from the reaction of LiCH(TMS)2 and PhNC
• Authors of publication: Fernandes, Manuel A.; Lappert, Michael F.; Layh, Marcus; Omondi, Bernard
• Journal of publication: Chemical Communications (Cambridge, United Kingdom)
• Year of publication: 2003
• Journal issue: 5
• Pages of publication: 656 - 657
• a: 12.4532 ± 0.0017 Å
• b: 12.473 ± 0.0017 Å
• c: 16.775 ± 0.002 Å
• α: 88.096 ± 0.003°
• β: 80.581 ± 0.003°
• γ: 61.552 ± 0.002°
• Cell volume: 2257.1 ± 0.5 ų
• Cell temperature: 173 ± 2 K
• Ambient diffraction temperature: 173 ± 2 K
• Number of distinct elements: 5
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.1473
• Residual factor for significantly intense reflections: 0.0834
• Weighted residual factors for significantly intense reflections: 0.2412
• Weighted residual factors for all reflections included in the refinement: 0.2775
• Goodness-of-fit parameter for all reflections included in the refinement: 1.081
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No