Information card for entry 7104036

Structure parameters

• Common name: (Tris(N,N'-(2,2')bipyridinyl-5,5'-diyl-bis-carbamic acid diethyl ester)iron(ii))-diperchlorate- dihydrate
• Chemical name: [Tris(N,N'-[2,2']bipyridinyl-5,5'-diyl-bis-carbamic acid diethyl ester)iron(II)]-diperchlorate- dihydrate
• Formula: C24 H29 Cl Fe0.5 N6 O11
• Calculated formula: C24 H27 Cl Fe0.5 N6 O11
• Title of publication: Large size anion binding with iron(II) complexes of a 5,5'-disubstituted-2,2'-bipyridine ligand
• Authors of publication: Wu, Biao; Yang, Xiao-Juan; Janiak, Christoph; Gerhard Lassahn, Paul
• Journal of publication: Chemical Communications (Cambridge, United Kingdom)
• Year of publication: 2003
• Journal issue: 7
• Pages of publication: 902 - 903
• a: 18.459 ± 0.005 Å
• b: 25.212 ± 0.006 Å
• c: 14.755 ± 0.004 Å
• α: 90°
• β: 117.34 ± 0.004°
• γ: 90°
• Cell volume: 6100 ± 3 ų
• Cell temperature: 223 ± 2 K
• Ambient diffraction temperature: 223 ± 2 K
• Number of distinct elements: 6
• Space group number: 15
• Hermann-Mauguin space group symbol: C 1 2/c 1
• Hall space group symbol: -C 2yc
• Residual factor for all reflections: 0.2067
• Residual factor for significantly intense reflections: 0.0871
• Weighted residual factors for significantly intense reflections: 0.2221
• Weighted residual factors for all reflections included in the refinement: 0.3067
• Goodness-of-fit parameter for all reflections included in the refinement: 1.01
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No