Information card for entry 7104113

Structure parameters

• Formula: C64 H104 Ga2 N8 Yb
• Calculated formula: C64 H104 Ga2 N8 Yb
• SMILES: [Yb]12([Ga]3N(C=CN3c3c(cccc3C(C)C)C(C)C)c3c(cccc3C(C)C)C(C)C)([Ga]3N(C=CN3c3c(cccc3C(C)C)C(C)C)c3c(cccc3C(C)C)C(C)C)([N](CC[N]1(C)C)(C)C)[N](CC[N]2(C)C)(C)C
• Title of publication: Gallyl lanthanide complexes containing unsupported Ln-Ga (Ln = Sm, Eu, Yb or Tm) bonds.
• Authors of publication: Jones, Cameron; Stasch, Andreas; Woodul, William D
• Journal of publication: Chemical communications (Cambridge, England)
• Year of publication: 2008
• Journal volume: 34
• Journal issue: 1
• Pages of publication: 113 - 115
• a: 21.866 ± 0.004 Å
• b: 14.06 ± 0.003 Å
• c: 21.602 ± 0.004 Å
• α: 90°
• β: 95.47 ± 0.03°
• γ: 90°
• Cell volume: 6611 ± 2 ų
• Cell temperature: 123 ± 2 K
• Ambient diffraction temperature: 123 ± 2 K
• Number of distinct elements: 5
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/c 1
• Hall space group symbol: -P 2ybc
• Residual factor for all reflections: 0.088
• Residual factor for significantly intense reflections: 0.0459
• Weighted residual factors for significantly intense reflections: 0.1029
• Weighted residual factors for all reflections included in the refinement: 0.1171
• Goodness-of-fit parameter for all reflections included in the refinement: 0.992
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No