Information card for entry 7104132

Structure parameters

• Formula: C4 H131.07 As6 Gd6 Na8 O398.07 W65
• Calculated formula: C4 As6 Gd6 Na8 O398.08 W65
• Title of publication: Polyoxotungstate-encapsulated Gd(6) and Yb(10) complexes.
• Authors of publication: Hussain, Firasat; Gable, Robert W; Speldrich, Manfred; Kögerler, Paul; Boskovic, Colette
• Journal of publication: Chemical communications (Cambridge, England)
• Year of publication: 2009
• Journal volume: 34
• Journal issue: 3
• Pages of publication: 328 - 330
• a: 23.0942 ± 0.0017 Å
• b: 25.6844 ± 0.0018 Å
• c: 31.749 ± 0.003 Å
• α: 66.23 ± 0.001°
• β: 83.185 ± 0.002°
• γ: 84.002 ± 0.002°
• Cell volume: 17080 ± 2 ų
• Cell temperature: 130 ± 2 K
• Ambient diffraction temperature: 130 ± 2 K
• Number of distinct elements: 7
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.1295
• Residual factor for significantly intense reflections: 0.0659
• Weighted residual factors for significantly intense reflections: 0.1369
• Weighted residual factors for all reflections included in the refinement: 0.1623
• Goodness-of-fit parameter for all reflections included in the refinement: 0.953
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No