Information card for entry 7104430

Structure parameters

• Formula: C47 H42 Cl5 N O P2 Ru
• Calculated formula: C47 H38 Cl5 N O P2 Ru
• Title of publication: Vinylidene rutheniums with an electrostructurally-flexible NO ligand and their ruthenacyclobutene formation.
• Authors of publication: Yamaguchi, Mamoru; Arikawa, Yasuhiro; Nishimura, Yoshimasa; Umakoshi, Keisuke; Onishi, Masayoshi
• Journal of publication: Chemical communications (Cambridge, England)
• Year of publication: 2009
• Journal volume: 34
• Journal issue: 20
• Pages of publication: 2911 - 2913
• a: 9.523 ± 0.003 Å
• b: 22.815 ± 0.007 Å
• c: 10.988 ± 0.002 Å
• α: 90°
• β: 103.112 ± 0.004°
• γ: 90°
• Cell volume: 2324.9 ± 1.1 ų
• Cell temperature: 298 ± 1 K
• Ambient diffraction temperature: 298 ± 1 K
• Number of distinct elements: 7
• Space group number: 11
• Hermann-Mauguin space group symbol: P 1 21/m 1
• Hall space group symbol: -P 2yb
• Residual factor for all reflections: 0.1348
• Residual factor for significantly intense reflections: 0.0703
• Weighted residual factors for significantly intense reflections: 0.1711
• Weighted residual factors for all reflections included in the refinement: 0.191
• Goodness-of-fit parameter for all reflections included in the refinement: 1.15
• Diffraction radiation wavelength: 0.7107 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No